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DIAGRAM ALIR PROSES PABRIK GLISEROL MONOOLEAT DARI GLISEROL DENGAN PROSES GLISEROLISIS METIL ESTER KAPASITAS 1.750 TON/TAHUN Keterangan Peralatan E-101 E-102 E-103 E-104 E-105 E-106 E-107 E-108 E-109 E-110 E-111 E-112 E-113 P-101A/B P-102A/B P-103A/B
Keterangan Gambar : lps hps cw
: Low Pressure Steam : High Pressure Steam : Cooling Water : Temperature, oC : Pressure, bar : Flow name
ME-Glycerol Preheater GMO Distillation Kondenser GMO Distillation Reboiler Heavy Liquid Distillation Kondenser Heavy Liquid Distillation Reboiler Low Quality GMO Kondenser Low Quality GMO Reboiler High Quality GMO Preheater High Quality GMO Kondenser High Quality GMO Reboiler High Quality GMO Product Cooler Recycle Stream Cooler Low Quality GMO Product Cooler Pompa Methyl Ester Pompa Glycerol Pompa Distillation Tower 102 Reflux
P-104A/B P-105A/B P-106A/B R-101 T-101 T-102 T-103 T-104 V-101 V-102 V-103 V-104 V-105 V-106 V-107 MF/UF/NF
Pompa Distillation Tower 101 Reflux Pompa Distillation Tower 103 Reflux Pompa Distillation Tower 104 Reflux Reaktor Glycerolisis Tower Distilasi Heavy Liquid Tower Distilasi GMO Mixture Tower Distilasi Low Quality GMO Tower Distilasi High Quality GMO Tangki Methyl Ester Tangki Glycerol Separator 3-Fase Heavy Liquid Reflux Vessel GMO Mixture Reflux Vessel Low Quality GMO Reflux Vessel High Quality GMO Reflux Vessel Makrofilter / Ultrafilter / Nanofillter
Keterangan Aliran Aliran-1 Aliran-2 Aliran-2A Aliran-2B Aliran-2C Aliran-2D Aliran-2E Aliran-2F Aliran-3A Aliran-3B Aliran-4 Aliran-5 Aliran-6A
Methyl Ester Crude Glycerol Filtrat Macrofilter Residu Macrofilter Filtrat Ultrafilter Residu Ultrafilter Filtrat Nanofilter Residu Nanofilter Mixed Feed Pre-heated Mixed Feed Keluaran Reaktor Heavy Liquid hasil pemisahan Vapor hasil pemisahan
Aliran-6B Aliran-7 Aliran-8 Aliran-9 Aliran-10 Aliran-11 Aliran-12 Aliran-13A/B Aliran-14A/B Aliran-15A/B Aliran-16 Aliran-17A/B
Light Liquid hasil pemisahan Campuran Umpan Tower Distilasi 102 Top Product Tower Distilasi 102 Glycerol yang di Recycle Top Product Tower Distilasi 101 Methyl Oleate yang di Recycle Campuran Umpan Tower Distilasi 103 Low Quality GMO (50%) Campouran Umpan Tower Distilasi 104 High Quality GMO (>96%) Glycerol & Methyl Oleate yang di Recycle Campuran Recycle Glycerol & Methyl Oleate
cw 130 1.3
cw
E-102
130 1.3
E-109 V-105
4
6A
7
LIC
V-107 V-103
LIC
R-101
E-111
20 1
Methyl Ester
130 1.3
3B
130 1.3
130 1.3
FIC
14B
T-104
V-101
FIC
hps
P-101 A/B
E-104
FIC
20
V-104
3A
1
E-101
E-103
16
cw
67.5 0.8
E-106
V-106 I-71
V-102
LIC
P-102 A/B
17B
FIC
20 1
MF
UF 2B
20 1
NF 2D
E-112
2F
cw 2A
2C
2E
LIC
P-104 A/B
cw
12
13A
E-105 FIC
11
20 1
cw
P-105 A/B
E-108
E-107 17A
13B 61 0.75
T-103
hps
278.5 1
Low Quality GMO
E-113
71 0.8
hps 287 1
260 1
E-110
9
P-106 A/B
10
T-101
2
LIC
20 1
hps
130 1 343 1
15B 200 0.8
P-103 A/B
cw
lps
Glycerol
15A
72 0.8
T-102
130 1.3
5
1
LIC
Hi-Quality GMO
cw
8
6B
237 1 14A
Neraca Massa
Unit
1
2
2A
2B
2C
2D
2E
2F
3A
3B
4
5
6A
6B
7
8
9
10
11
12
13A
13B
14A
14B
15A
15B
16
17A
17B
C
20
20
20
20
20
20
20
20
20
130
130
130
130
130
130
72
343
68
287
71
61
20
236,5
130
200
20
260
278,5
20
bar
1
1
1
1
1
1
1
1
1
1,3
1,3
1,3
1,3
1,3
1,3
0,8
1
0,8
1
0,8
0,75
1
1
1
0,8
1
1
1
1
GMO
kg/h
0
0
0
0
0
0
0
0
6,21
6,21
205,98
11,72
72,56
121,71
194,26
193,76
0,50
11,71
0
205,47
46,88
46,88
158,59
158,59
152,89
152,89
5,70
6,21
6,21
GDO
kg/h
0
0
0
0
0
0
0
0
2,54
2,54
6,87
0,08
1,48
5,31
6,79
4,51
2,28
0,076
0
4,59
2,75
2,75
1,83
1,83
1,57
1,57
0,27
2,55
2,55
Gliserol
kg/h
28,85
28,94
0,29
28,65
0,57
28,08
0,56
27,51
185,61
185,61
133,37
125,13
0,11
8,13
8,24
8,24
0,00
2,861
122,27
11,10
0
0
11,10
11,10
4,14
4,14
6,97
129,34
129,34
Air
kg/h
0,55
3,88
0,04
3,84
0,19
3,65
0,37
3,29
3,84
3,84
3,84
2,38
1,31
0,15
1,46
1,46
0,00
2,383
0
3,84
3,84
3,84
0
0
0
0
0
0
Metanol
kg/h
22,20
0,28
0,0028
0,28
0,01
0,27
0,01
0,27
22,46
22,46
40,86
8,72
28,53
3,62
32,15
32,15
0,00
8,715
0
40,86
40,86
40,86
0,0014
0,0014
0,0014
0
0
0
Metil Oleat
kg/h
170,355
0
0
0
0
0
0
0
298,79
298,79
128,54
2,04
0,05
126,45
126,50
6,50
119,99
2,040
0
8,54
0
0
8,54
8,54
0,10
0,10
8,44
128,44
128,44
Abu
kg/h
0
2,12
2,12
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Asam Lemak
kg/h
0
0,07
0,0007
0,07
0,02
0,05
0,05
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Total
kg/h
221,96
35,29
2,45
32,84
0,79
32,05
0,98
31,07
519,46
519,46
519,46
150,06
104,04
265,36
369,40
246,62
122,78
27,79
122,27
274,41
94,34
94,34
180,07
180,07
158,69
158,69
21,38
266,43
266,43
Temperature Pressure
o
Mass Flow :
Neraca Energi Nama Alat
Deskripsi
Heat Flow (kJ/h)
E-101
ME-Glycerol Preheater
1,431 x 105
E-102
GMO Distillation Condenser
4,911 x 105
E-103
GMO Distillation Reboiler
4,973 x 105
E-104
Heavy Liquid Distillation Condenser
1,017 x 105
E-105
Heavy Liquid Distillation Reboiler
1,553 x 105
E-106
Low Quality GMO Condenser
4,206 x 105
E-107
Low Quality GMO Reboiler
4,688 x 105
E-108
High Quality GMO Preheater
3,482 x 104
E-109
High Quality GMO Condenser
1,089 x 105
E-110
High Quality GMO Reboiler
1,343 x 105
E-111
High Quality GMO Product Cooler
4,146 x 104
E-112
Recycle Stream Cooler
2,055 x 105
E-113
Low Quality GMO Product Cooler
9,056 x 103
V-103
Separator 3 Fase
3.03 x 109
R-101
Reaktor Gliserolisis Metil Ester
2.8 x 105
0 0,0014
